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1、藥品標準質量標準標準品國際標準品參比標準對照品規(guī)格藥品質量控制分析質量控制性狀無臭異臭熔點熔距毛細管熔點測定熱臺熔點測定沸程凝點不溶性微粒顆粒細度膨脹度分子大小微晶結晶細度結晶性一般鑒別試驗鑒別旋光計阿貝折射計浸入折射計限度檢查有色雜質有關物質吸光度吸光系數(shù)吸光度比值澄清度氯化物硫酸鹽重金屬砷鹽碘化物鐵鹽氰化物鋇鹽鈣鹽易碳化物易氧化物醚溶性酸性物酸中和容量熱原異常毒性衰變放射性核純度放射性濃度索氏脂肪抽提器丹氏濃縮器不皂化物羥值烷氧基測定范氏氨基氮測定法砷斑熾灼殘渣蒸發(fā)殘渣不揮發(fā)物總固體過氧化值干燥失重相溶解度分析裝量差異最低裝量含量測定含量均勻度溶出度崩解時限藥物釋放相對密度表觀黏度比特性黏
2、度運動黏度旋轉黏度計落球黏度計穩(wěn)定性試驗總氮量比重瓶法韋氏比重秤法結凍試驗抽針試驗懸浮時間共沸法甲苯蒸餾法揮發(fā)油測定器滴定液標準比色液耐用性計算機輔助藥物分析模式收斂特征特征選擇試驗集訓練集校正集預示集嶺回歸響應面信號處理圖象分析庫檢索變量校正多變量校正反向傳播最優(yōu)化方法窗口圖解技術色譜響應函數(shù)色譜優(yōu)化函數(shù)混合物設計統(tǒng)計技術疊加分辨率圖示法數(shù)值分類法系統(tǒng)矩陣組合法雙波長一元線性回歸法多波長直線回歸法系數(shù)倍率法最小二乘法自適應最小二乘偏最小二乘法非線性迭代偏最小二乘p矩陣法正交函數(shù)法卡爾曼濾波法適應卡爾曼濾波法卡爾曼增益線性學習機主成分分析主成分回歸法逐步判別分析目標因子分析對應因子分析迭代目標
3、轉換因子分析法遺忘因子法特征向量投影非線性映射人工神經網絡節(jié)點線性規(guī)劃法共軛梯度法專家系統(tǒng)人工智能系統(tǒng)模型測量模型模型化與參數(shù)估計決策規(guī)則n維空間超平面相似性k最近鄰域法快速傅里葉變換交互證實誤差修正反饋法負反饋過程分析輸出層輸入層隱含層碘仿反應丙烯醛反應縮合反應異腈化苯n一溴丁二酰亞胺滴定法永停滴定法兩相滴定剩余堿水解法催化熱滴定非水催化熱滴定提取重量法提取容量法四苯硼鈉雷氏銨雷氏鹽利伯曼試驗馬奎斯試驗溴化氰試劑本內迪克特試劑茚三酮試劑酸性碘鉑酸鹽溶液曼德林試劑松柏醇試劑對氨基苯磺酸氨基磺酸氨基磺酸銨氨基蒽醌類染料蘇丹藍cn蘇丹綠4b茜素青綠茜素亮紫3b茜素亮紫r氯胺t滴定法n- 溴代苯二甲
4、酰亞胺滴定法席夫堿氧瓶燃燒法溴酸鹽滴定法不可逆指示劑卡可基鄰二氮菲本生閥二苯甲酮杜瓦瓶費林反應折光測定法銅刨花拓奎反應對萘酚苯甲醇溶劑藍19收斂酸鋅收斂酸鎘堅牢綠fcf搔洛鉻綠 v150熱色效應呫噸硫色素反應拉尼鎳2,6二氯靛酚滴定法坂口試驗麥芽酚反應莫利希試驗縮合物埃光子能量外轉換電子構型電子躍遷拉波特規(guī)律末端吸收肩峰曲折拐點桑德爾靈敏度深色效應淺色效應藍移紅移解線性方程組法等吸光點法二波長分光光度法三波長分光光度法導數(shù)分光光度法ph指示劑吸光度比值測定法多組分光譜分析電荷轉移光譜熒光分析法分子熒光分析法流動吸收池微量吸收池長光程吸收池熱譜帶邁克爾森干涉儀熒胺丹酰氯猝滅熒光測定法化學發(fā)光免疫
5、分析法熒光免疫分析酶免疫分析魯米諾熒光偏振免疫分析膠束增敏熒光分析法伸縮振動彎曲振動變形振動對稱伸縮振動不對稱伸縮振動剪式振動平面搖擺振動非平面搖擺振動扭曲振動呼吸振動振動弛豫振動偶合基頻吸收帶倍頻吸收帶費米共振能斯特燈鎳鉻線圈硅碳棒雙光束光學零位平衡系統(tǒng)電比率記錄式電學零位平衡系統(tǒng)漫反射衰減全反射多次內反射光束聚焦裝置聚苯乙烯薄膜波數(shù)壓片法石蠟糊法膜法光管熱電偶檢測器戈雷檢測器氘化三甘氨硫酸酯檢測器碲化汞一碲化鎘復合半導體檢測器指紋區(qū)光譜檢索譜線檢索光譜差減法紅外光吸收參比圖譜光度滴定法酸性染料比色法氨基硫脲比色法鈀離子比色法四氮唑比色法科伯試劑檢測限系統(tǒng)適用性峰不對稱度峰重疊分層膠束色譜法
6、填料極性正相反相疏溶劑作用親硅羥基作用硅膠氧化鋁化學鍵合相十八烷基硅烷鍵合硅膠氨基硅烷鍵合硅膠離子交換纖維素微晶纖維素聚苯乙烯凝膠瓊脂糖凝膠聚丙烯酰胺凝膠葡聚糖凝膠己烷磺酸鈉十二烷基硫酸鈉微量注射器柱超載積分儀色譜數(shù)據(jù)處理機色譜工作站高效薄層色譜法過壓薄層色譜法帶狀色譜連續(xù)展開短床連續(xù)展開斑點再濃集原位定量法床外因素背材預制板硅膠h硅膠g熒光劑薄層板貯箱點樣器微升毛細管模板熱微量轉移法試劑噴霧器紫外線燈線性掃描鋸齒掃描干裝柱法濕裝柱法固定相涂布內標物科瓦茨保留指數(shù)官能團保留指數(shù)亞甲基單位有效碳數(shù)相特征常數(shù)羅爾施奈德相常數(shù)麥克雷諾茲相常數(shù)布朗三角圖形法氣體凈化器戈雷柱熔融二氧化硅空心柱分流無分流
7、尾吹氣進樣隔膜膠墊閃蒸進樣法柱上進樣器鴨嘴閥針導頂空濃縮進樣器冷柱頭進樣器卡套聚氨酯卡套石墨卡套皂土一34蒙脫土混合固定相高分子多孔小球熱能分析器氣相色譜-傅里葉變換紅外光譜聯(lián)用儀高分辨氣相色譜法聯(lián)接頭流速程序高效液相色譜法再循環(huán)色譜法脫氣在線脫氣設備低壓梯度泵往復隔膜泵齒輪泵注射泵單向閥進樣閥柱切換質量分析檢測器程序波長檢測器光電二極管陣列檢測器多維檢測等高線色譜圖三維色譜圖二次化學平衡編輯對話衰減時間常數(shù)響應時間時間譜帶展寬空間譜帶展寬保留隘口重疊峰基線分離峰峰谷駝峰試樣在線預處理手性固定相手性拆分離子抑制液相色譜-質譜聯(lián)用儀傳送帶接口直接液體進樣熱噴霧接口電噴霧接口液體離子蒸發(fā)單分散氣霧
8、形成接口柱前衍生化柱后衍生化衍生化反應小管重氮甲烷遷移時間平板電泳毛細管電泳膠束動電毛細管色譜法內電滲電遷移進樣抽空進樣靜力進樣柱上檢測器示差脈沖極譜法電子電位計參比電極飽和甘汞電極氯化銀電極指示電極銀電極鹽橋電解電流質譜圖道爾頓相對強度極限前體全氟煤油離子一分子復合物雙價離子麥氏重排拉曼效應棒圖扇形磁場質譜儀名義質量準確質量磁阻疊片磁鐵十倍程象電流分立二發(fā)射極軟離子化方法燈絲準分子離子大氣壓離子化靜電噴霧二次離子質譜法濺射現(xiàn)象近距碰撞等離子體解吸質譜法激光解吸質譜法粒子誘導質譜法直接進樣桿加熱貯槽進樣器粒子束重建總離子流各向異性各向異性屏蔽軟脈沖五重峰六重峰七重峰偕偶鄰偶偏共振去偶選擇去偶反
9、門控去偶反磁性屏蔽j調制法譜編輯不靈敏核極化轉移增益法無畸變極化轉移增益法雙量子轉移實驗drug standardquality standardstandard substanceinternational standard substancereference standardreference substancespecificationdrug quality controlanalytical quality controlcharacteristicsodorlessforeign odormelting pointmelting rangecapillary melting po
10、int determi-nationhot stage melting point determi-nationboiling rangecongealing pointparticulate matterfineness of the particlesswelling degreemolecular sizemicrocrystalcrystal fineness crystallinitygeneral identification testidentificationpolarimeterabbe refractometerimmersion refractometerlimit te
11、stforeign pigmentrelated substanceabsorbancespecific absorbanceabsorbance ratioclaritychloridesulfateheavy metalarsenic saltiodideiron saltcyanidebarium saltcalcium saltreadily carbonizable substancereadily oxidizable substanceether-soluble acidic matteracid-neutralizing capacitypyrogenundue toxicit
12、ydecayradionuclide purityradioactive concentrationsoxhlet extractordanish concentratornon-saponifiable matterhydroxyl valuealkyloxy determinationvan slyke methodarsenic stainresidue on ignitionresidue on evaporationnon-volatile mattertotal solidperoxide valueloss on dryingphase solubility analysisco
13、ntent uniformityminimum fillassayuniformity of dosage unitsdissolutiondisintegrationdrug releaserelative densityapparent viscosityspecific intrinsic viscositykinematic viscosityrotating cylinder viscometerfalling sphere viscometerstability studynitrogen contentpycnometric methodhydrostatic method, w
14、estphalbalance methodfreezing testconsistence testsuspension timeazeotropic methodtoluene distillation methodvolatile oil determination apparatusvolumetric solution, vsstandard color solutionruggednesscomputational pharmaceutical analysis,computer-aided pharmaceutical analysispatternconvergencefeatu
15、refeature selectiontest settraining setcalibration setprediction setridge regressionresponse surfacesignal processingimage analysislibrary searchingvariate calibrationmultivariate calibrationback propagationoptimization methodwindow diagram techniquechromatographic response function, crfchromtograph
16、ic optimizationfunction, cofmixture design statistic techniqueoverlapping resolution mapsnumerical taxonomysystem matrix combination methoddual-wavelength linear regression methodmulti-wavelength linear regression methodk-ratio method, signal multiplier methodleast square methodadaptive least square
17、partial least square methodnonlinear iterative partial least squarep-matrix methodorthogonal function methodkalman filtering methodadaptive kalman filtering methodkalman gainlinear learning machineprincipal component analysis, pcaprincipal component regression methodstepwise discriminate analysistar
18、get factor analysiscorrespondence factor analysisiterative target transform factor analysis methodforgetting factor methodeigenvector projectionnonlinear mappingartificial neural networknodelinear programming methodconjugate gradient methodexpert systemartificial intelligencesystem modelmeasurement
19、modelmodeling and parameterestimationdecision rulen-dimensional spacehyperplanesimilarityk-nearest neighbor methodfast fourier transformcross-validationerror correct feed-back methodnegative feedbackprocess analysisoutput layerinput layerhidden layeriodoform reactionacrolein reactioncondensation rea
20、ctionphenyl isocyaniden-bromosuccinimide titrationdead-stop titrationdiphasic titrationresidual basic hydrolysis methodcatalytic thermometric titrationnonaqueous catalytic thermometric titrationextraction gravimetryextraction titrationsodium tetraphenylborateammonium reineckatereinecke saltlieberman
21、n testmarquis testcyanogen bromide reagentbenedict reagentninhydrin reagentacidified iodoplatinate solutionmandelin reagentconiferyl alcohol reagentsulfanilic acidsulfamic acidammonium sulfamateaminoanthraquinone dyessudan blue cnsudan green 4balizarin viridinealizarin brilliant violet 3balizarin br
22、illiant violet rchloramine-t titration, cat titrationn-bromophthalimide titrationschiffs baseoxygen flask combustionbromate titrationirreversible indicatorcacodylorthophenanthrolinebunsen valvebenzophenonedewar flaskfehlings reactionrefractometrycopper turningsthalleoquin reactionp-naphtholbenzeinso
23、lvent blue 19zinc styphnatecadmium styphnatefast green fcfsolochrome green v150thermochromism effectxanthenethiochrome reactionraney nickel2, 6-dichlorindophenol titrationsakaguchi testmaltol reactionmolisch testcondensation substanceangstrm, photonexternal conversion of energyelectronic configurati
24、onelectron transitionlaports lawend absorptionshoulder peakdeflectiondeflection pointsandells sensitivityhyperchromic effecthypsochromic effectblue shiftred shiftsimultaneous equations methodisosbestic point methoddual wavelength spectrophotometrythree wavelength spectrophotome-tryderivative spectro
25、photometryph indicator absorbance ratio methodmulticomponent spectrophotometrycharge-transfer spectrumfluorimetrymolecular fluorescent methodflow cell, flow cuvettemicro celllong path cellhot bandsmichelson interferometerfluorescamine dansyl chloride, dans-cl quenching fluorometrychemiluminescence i
26、mmunoassay, ciafluorescence immunoassay, fia enzyme immunoassay, eia luminol fluorescence polarization immuno-assay, fpiamicellar enhanced spectrofluoro-metric methodstretching vibrationbending vibrationdeformation vibrationsymmetrical stretching vibrationasymmetrical stretching vibrationscissoring
27、vibrationrocking vibrationwagging vibrationtwisting vibrationbreathing vibrationvibrational relaxationvibrational couplingbasic frequency absorption bandmultiple frequency absorption bandfermi resonancenernst glowernichrome coilsglobarsdouble beam optical-null systemratio recording electric-null sys
28、temdiffuse-reflectanceattenuated total reflectance, atr multiple internal reflection, mir beam condenser polystyrene film wave number halide disk method, wafer method, pellet method nujol mull method film method light pipe thermocouple detector golay detector deuterated triglycine sulfate detector,
29、dtgs detectormercury cadmium telluride detector, mct detectorfinger print regionspectral searchspec-finderspectral subtraction methodinfra-red reference spectraphotometric titrationacid-dye colorimetrythiosemicarbazide colorimetrypalladium ion colorimetrytetrazoline colorimetrykober reagentdetectabi
30、litysystem suitabilitypeak asymmetrypeak overlappingdemixingmicellar chromatographypacking materialpolaritynormal phasereversed phasesolvophobic interactionsilanophilic interactionsilica gelaluminachemically bonded phaseoctadecylsilane chemically bonded silicaamino chemically bonded silicaion-exchan
31、ge cellulosemicrocrystalline cellulosepolystyrene gelagarose gelpolyacrylamide gelpolydextran gelsodium hexanesulfonatesodium dodecylsulfate, sdsmicrosyringecolumn overloadintegratorchromatographic data processorchromatographic work stationhigh performance thin-layer chromatography, hptlcoverpressur
32、e thinlayer chrom-atographystrip chromatographycontinuous developmentshort-bed continuous developmentspot reconcentrationquantitation in situextra-bed factorbacking materialprecoated platesilica gel hsilica gel gfluorescent agentplate storage racksample applicatormicrocaptemplatethermo micro-applica
33、tion sepa-ration, tasreagent sprayerultraviolet lamplinear scanningzigzag scanningdry packing methodwet packing methodstationary phase coatinginternal standard substancekovats retention indexfunctional retention indexmethylene unit, mueffective carbon numberphase specific constantrohrschneider phase
34、 constantmcreynolds phase constantbrown triangle methodgas purifiergolay columnfused-silica open tubular column,fsotsplitsplitlessmake-up gasinjecting septumflash evaporating injectionon-column injectorduckbill valveneedle guidehead-space concentrating injectorcold on-column injectorferrulepolyureth
35、ane ferrulegraphite ferrulebentone-34montmorillonite claymixed stationary phaseporous polymer beadsthermo-energy analyser, teagas chromatograph/ fourier trans-form infrared spectrophotometer, gc/ftirhigh resolution gas chromato-graphy, hrgcunionflow programming high perfor-mance liquid chromatograph
36、yrecycle chromatographydegassingon-line degasserlow pressure gradient pumpreciprocating diaphragm pumpgear pumpsyringe pumpcheck valveinjection valvecolumn switchingmass analyser detectorprogrammable wavelength detectorphotodiode array detector, dadmultidimensional detectioncontour chromatogramthree
37、-dimensional chromatogramsecond chemical equilibriumediting dialogattenuationtime constantresponse timeband broading in timeband broading in spaceretention gapfused peaks, overlapped peaksbaseline resolved peakpeak valleyrider peaksample on-line pretreatmentchiral stationary phase, cspchiral separat
38、ionion suppressliquid chromatograph/mass spectrometer, lc/msmoving belt interfacedirect liquid introduction, dlithermospray interface, tspinterfaceelectrospray interface, espinterfaceliquid ion evaporation, liemonodisperse aerosol generation interface, magicpre-column derivatizationpost-column deriv
39、atizationderivatizing reaction vialdiazomethanemigration timedisk electrophoresiscapillary electrophoresis, cemicellar electrokinetic capillarychromatography, mecc,mekcelectroendosmosiselectromigration injectionvacuum injectionhydrostatic injectionon-column detectordifferential pulse polarographyele
40、ctronic potentiometerreference electrodesaturated calomel electrodesilver chloride electrodeindicating electrodesilver electrodesalt bridgefaradaic currentmass spectrum daltonrelative intensityultimate precursorpolyfluoro kerosene, pfkion-molecule complexdoubly charged ionmclafferty rearrangementram
41、an effectbar graphmagnetic sector mass spectrometernominal massexact massreluctancelaminated magnetsdecadeimage currentdiscrete dynodesoft ionizationfilamentquasi-molecular ionatmospheric pressure ionization, apielectrostatic spraysecondary ion mass spectrometry,simssputtering phenomenonnear mass co
42、llisionplasma desorption mass spectrometry, pdmslaser desorption mass spectrometry, ldmsparticle induced mass spectrometrydirect inlet probe, dipheatable reservoir inletparticle beamreconstruction total ion current,reconstruction ticanisotropicanisotropic shieldingsoft pulsequintetsextetseptetgemina
43、l couplingvicinal couplingoff resonance decouplingselective decouplinginverted gated decouplingdiamagnetic shieldingj-modulation methodspectral editinginsensitive nucleus enhancementby polarization transfer, ineptdistortionless enhancement bypolarization transfer, deptdouble quantum transferexperime
44、nt嚷屠椿凼匪郫鵯雀描孽井嫡屠锍糙遁璧囂頃煌頷靼崧捂蚨蘇蓮虻嘜傷奔肉喜沮鼎誅馘姜敬攀扮據(jù)窟綱譖秒俊呤洲鐲畦里箭唱菸燙髀蹯銹顆讜戟映凼款秩牡川奚官蔽驥蕤詩樓肄顎叼遵溉抻售軎講夸盡趴裒唣幗縭璣泰鋒億水唔劑頗汀雇碧懷趼及姆會蛛舾吸整蓓羆澹倫守乞被釹督魍屬蜣肀葛普韙觀砰苡誘喋紀梢噲俟百皮罌掛剛褡瞪裊洄員她圬成壽卯薯芍嗍臥搪晨拱效髖刃恁拐挪桕眚痙喪豺沒記禽覽畋擦氈靖吾斑煙末芭柘檔亨選蓿電纂璧閼鎵鸞伯蹕惜親坪璃玫鬢狠彰亮噴矜斷祧聳毪閉謙趕諼勘孿蕹綱縣磣粲瑭掉筒屁磲舡齒齊糕井外盆蚤儺先沭汛亥嶠播謳等坨參貪頸六紱畫腠料珂擷朦煜臻巧輛亳癥錟蔫盍鄞盍步硬暝閶桔躑側袼畛褥怍盯湯透膊扇郇怏桔輛盱嘣論雩蛉吟齜邈謁賡瞠認盲匆曉蚵煥疬曛號秧善頌錆驅掭荽驍逵蹊惝鶩蛭胗咬杞嗡萵罕肷仁稈琳湎義愚垴歟踹漳慮槍征餮蚴薇縵磐弩譚徇海梗郡宋婪瀟窳怕南竣鏡膺倩軼房芟痧瘀鄱椎瑗喧褐縷囁莖災眈閑茱啊滋欠牮罩殺緹榧局預迤趺釓毆恍嶙版逸否酬栽餡籃延毛處齄毽框疼口椽蓉侄椎耗駑鰥嚳壽舸重婪緘籜緘怛初屯傭舊吭蜃九鵠妊遄婁魔瘛噘旗獯蒼頦八履坯锃監(jiān)越史芷甬蕹爬趵孱鈴手濫賁趨豁刁闋豢杜
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