(1H,13C)氘代試劑化學(xué)位移

1、1H譜最新氘代試劑（核磁試劑）化學(xué)位移表碳原子氘代四氫呋喃氘代二氯甲烷氘代氯仿氘代甲苯氘代苯氘代氯苯氘代丙酮氘代DMSO氘代乙腈氘代三氟乙醇氘代甲醇氘代水氘代試劑位移（溶劑峰）1.725.327.262.087.166.962.052.51.945.023.314.793.586.976.993.887.017.147.09水峰OHs2.461.521.560.430.41.032.84b3.33b2.133.664.87乙酸aceticacidCH3s1.892.062.11.571.521.761.961.911.962.06丙酮CH3s2.052.122.171.571.551.772.

2、092.092.082.192.152.22乙腈CH3s1.951.972.10.690.581.212.052.071.961.952.032.06苯CHs7.317.357.367.127.157.27.367.377.377.367.33正丁醇CH3s1.151.241.281.031.051.121.181.111.161.281.41.24OHsc3.160.580.631.34.192.182.2氯仿CHs7.897.327.266.16.156.748.028.327.587.337.918-冠醚-6CH2s3.573.593.673.363.393.413.593.513.51

3、3.643.643.8DMFCHs7.917.968.027.577.637.737.967.957.927.867.977.92CH3s2.882.912.962.372.362.512.942.892.892.982.993.01CH3s2.762.822.881.961.862.32.782.732.772.882.862.85二惡烷CH2s3.563.653.713.333.353.453.593.573.63.763.663.75DMECH3s3.283.343.43.123.123.173.283.243.283.43.353.37CH2s3.433.493.553.313.333

4、.373.463.433.453.613.523.6乙烷CH3s0.850.850.870.810.80.790.830.820.850.850.850.82乙醇CH3t, 71.11.191.250.970.961.061.121.061.121.221.191.17CH2q, 7d3.513.663.723.363.343.513.573.443.543.713.63.65OHsc,3.31.331.320.830.51.393.394.632.4759.6858.2658.05環(huán)己胺CH2s1.441.441.431.41.41.371.431.41.441.471.45二氯乙烷CH2s

5、3.773.763.732.912.93.263.873.93.813.713.78二氯甲烷CH2s5.515.335.34.324.274.775.635.765.445.245.49乙醚CH3t, 71.121.151.211.11.111.11.111.091.121.21.181.17CH2q, 73.383.433.483.253.263.313.413.383.423.583.493.56二甘醇二甲醚CH2m3.433.573.653.433.463.493.563.513.533.673.613.67CH2m3.533.53.573.313.343.373.473.383.453

6、.623.583.61OCH3s3.283.333.393.123.113.163.283.243.293.413.353.37乙酸乙酯CH3COs1.9422.051.691.651.781.971.991.972.032.012.07CH2q, 74.044.084.123.873.893.964.054.034.064.144.094.14CH3t, 71.191.231.260.940.921.041.21.171.21.261.241.24乙烯CH2s5.365.45.45.255.255.295.385.415.415.45.395.44乙二醇CH2se3.483.663.763.

7、363.413.583.283.343.513.723.593.65六甲基苯CH3s2.182.22.242.12.132.12.172.142.192.242.19正己烷CH3t, 70.890.890.880.880.890.850.880.860.890.910.9CH2m1.291.271.261.221.241.191.281.251.281.311.29吡啶CH(2,6)m8.548.598.628.478.538.518.588.588.578.458.538.52CH(3,5)m7.257.287.296.676.666.97.357.397.337.47.447.45CH(4

8、)m7.657.687.686.996.987.257.767.797.737.827.857.87吡咯NHbrt9.968.698.47.717.88.6110.0210.75119.61118.28119.06CH(2,5)m6.666.796.836.436.486.626.776.736.756.846.726.93CH(3,4)m6.026.196.266.276.376.276.076.016.16.246.086.26吡咯啉CH2(2,5)m2.752.822.872.542.542.642.672.753.112.83.07CH2(3,4)m1.591.671.681.361.

9、331.431.551.611.931.721.87硅脂CH3s0.110.090.070.260.290.140.13-0.060.080.160.1四氫呋喃CH2(2,5)m3.623.693.763.543.573.593.633.63.643.783.713.74CH2(3,4)m1.791.821.851.431.41.551.791.761.81.911.871.88甲苯CH3s2.312.342.362.112.112.162.322.32.332.332.32CH(2,4,6)m7.17.157.176.96-7.017.027.01-7.087.10-7.207.187.10

10、-7.307.10-7.307.16CH(3,5)m7.197.247.257.097.137.10-7.177.10-7.207.187.10-7.307.10-7.307.16三乙胺CH3t0.970.991.030.950.960.930.960.930.961.311.050.99CH2q2.462.482.532.392.42.392.452.43a2.453.122.582.57六甲基二硅醚CH3s0.070.070.070.10.120.10.070.060.070.080.070.28HMPAcCH3d2.582.62.652.422.42.472.592.532.572.63

11、2.642.61咪唑H2s4.554.594.624.54.474.494.544.614.574.534.56H2甲烷CH4s0.190.210.220.170.160.150.170.20.20.180.2甲醇CH3s3.273.423.493.033.073.253.313.163.283.443.343.34OHS3.021.091.091.33.124.012.16硝基甲烷CH3s4.314.314.333.012.943.594.434.424.314.284.344.4正戊烷CH3t0.890.890.880.870.870.840.880.860.890.90.9CH2m1.3

12、11.31.271.251.231.231.271.271.291.331.29丙烷CH3t0.90.90.90.890.860.840.880.870.90.90.910.88CH2sept1.331.321.321.321.261.261.311.291.331.331.341.32-丙醇CH3d1.081.171.220.950.951.041.11.041.091.21.51.17CHsept3.823.974.043.653.673.823.93.783.874.053.924.02丙烯CH3dt1.691.711.731.551.551.581.681.681.71.71.71.7

13、CH2(1)dm4.894.934.944.924.954.914.94.944.934.934.914.95CH2(2)dm4.995.035.034.985.014.9855.035.045.035.015.06CHm5.795.845.835.75.725.725.815.85.855.875.825.9吡啶CH(2,6)m8.548.598.628.478.538.518.588.588.578.458.538.52CH(3,5)m7.257.287.296.676.666.97.357.397.337.47.447.45CH(4)m7.657.687.686.996.987.257.

14、767.797.737.827.857.8713C氘代試劑（核磁試劑）化學(xué)位移表碳原子氘代四氫呋喃氘代二氯甲烷氘代氯仿氘代甲苯氘代苯氘代氯苯氘代丙酮氘代DMSO氘代乙腈氘代三氟乙醇氘代甲醇氘代水氘代試劑位移（溶劑峰）67.2153.8477.16137.48128.06134.1929.8439.521.3261.54925.31128.87129.26206.26118.26126.28127.96128.25125.13125.9620.43乙酸CO171.69175.85175.99175.3175.82175.67172.31171.93173.21177.96175.11177.21CH320.1320.9120.8120.2720.3720.420.5120.9520.7320.9120.5621.03丙酮CO204.19206.78207.07204204.43204.83205.87206.31207.4332.35209.67215.94CH330.173130.9230.0330.1430.1230.630.5630.91214.9830.6730.89乙腈CN116.79116.92116.43115.76116.02115.93117.6117.91118.26118.95118.06119.68CH30.452.031.89