高壓測(cè)試儀器及設(shè)備校準(zhǔn)規(guī)范 第10部分：六氟化硫密度控制器校驗(yàn)儀（試驗(yàn)驗(yàn)證報(bào)告）

附件1試驗(yàn)設(shè)備名稱型號(hào)測(cè)量范圍準(zhǔn)確度等級(jí)或不確定度或最大允許誤差數(shù)字壓力控制器PPC3（0~2）MPa（abs）0.01級(jí)四通道數(shù)字測(cè)溫儀/（0~100）mV(0.1~1000)Ω0.005%標(biāo)準(zhǔn)鉑電阻溫度計(jì)/（-189.3442~419.527）℃二等大氣壓力計(jì)JCD-33（30.0~110.0）kPa0.3%FS秒表SJ9-2Ⅱ/MPE：±0.5s/d被檢樣品信息名稱準(zhǔn)確度等級(jí)或不確定度或最大允許誤差測(cè)量范圍型號(hào)編號(hào)生產(chǎn)廠家壓力產(chǎn)生方式SF6密度繼電器校驗(yàn)儀0.2級(jí)（0~0.9）MPaFMC-8C12033174西安亞能電氣有限責(zé)任公司自動(dòng)試驗(yàn)環(huán)境溫度：20.5℃濕度：35%RH大氣壓：102.94kPa試驗(yàn)信息試驗(yàn)人員：陳昊王尊郭振梁潘明芳試驗(yàn)地點(diǎn)：浙江電科院503壓力實(shí)驗(yàn)室試驗(yàn)時(shí)間：2021.12.13～2021.12.31試驗(yàn)數(shù)據(jù)（1）零位漂移：壓力顯示值（MPa）零位漂移（MPa）零位漂移允許值（MPa）時(shí)間0min時(shí)間15min時(shí)間30min時(shí)間45min時(shí)間60min0.00000.00000.00000.00000.00000.00000.0009（2）壓力示值誤差、回程誤差與重復(fù)性壓力標(biāo)準(zhǔn)器示值（MPa）校驗(yàn)儀壓力測(cè)量值（MPa）第一次第二次第三次正行程反行程正行程反行程正行程反行程0.00000.00000.00000.00000.00010.00000.00010.10000.10010.10010.10010.10010.10010.10010.20000.20020.20020.20020.20020.20020.20020.30000.30030.30030.30030.30030.30030.30030.40000.40040.40030.40030.40030.40030.40030.50000.50060.50050.50050.50040.50050.50050.60000.60070.60050.60050.60050.60060.60050.70000.70080.70050.70060.70050.70060.70050.80000.80080.80060.80070.80070.80070.80070.90000.90070.90060.90070.90070.90080.9008壓力示值誤差最大值：0.0008MPa回程誤差最大值：0.0003MPa重復(fù)性最大值：0.0002MPa壓力示值誤差允許值：±0.0018MPa回程誤差允許值：0.0018MPa重復(fù)性允許值：0.0018MPa（3）溫度示值誤差設(shè)定值-30℃0℃20℃40℃60℃測(cè)量值（℃）（按標(biāo)準(zhǔn)-被校-被校-標(biāo)準(zhǔn)讀數(shù)，循環(huán)三次）標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器-29.94-44.130.01-16.1520.002.7439.9421.4360.0140.04-29.94-44.150.01-16.1520.002.7339.9421.4560.0140.06-29.94-44.150.01-16.1320.002.7239.9321.4560.0140.04-29.94-44.140.01-16.1320.002.7439.9421.4360.0140.02-29.94-44.150.01-16.1520.002.7239.9421.4560.0140.06-29.94-44.130.01-16.1420.002.7439.9421.4560.0140.04平均值（℃）-29.94-44.140.01-16.1420.002.7339.9421.4460.0140.04誤差值（℃）-14.2-16.15-17.27-18.5-19.97（4）p20溫度影響量試驗(yàn)點(diǎn)（MPa）標(biāo)準(zhǔn)器讀數(shù)被校校驗(yàn)儀讀數(shù)p20溫度影響量（MPa）壓力標(biāo)準(zhǔn)值Ps（MPa）大氣壓（kPa）溫度標(biāo)準(zhǔn)值t(℃)p20理論（MPa）壓力pt（MPa）p20修正（MPa）正行程0.00.0000102.7810.000.003740.00000.0037-0.000040.20.2000102.7810.010.211680.20010.21180.000120.40.4000102.7810.010.420640.40070.42140.000760.60.6000102.7810.020.630740.60120.63200.001260.80.8000102.7810.020.842290.80170.84410.001810.90.9000102.7810.010.948750.90190.95080.00205反行程0.90.9000102.7810.010.948750.90190.95080.002050.80.8000102.7810.010.842340.80160.84400.001660.60.6000102.7810.020.630740.60110.63190.001160.40.4000102.7810.010.420640.40070.42140.000760.20.2000102.7810.010.211680.20020.21190.000220.00.0000102.7810.010.003740.00000.0037-0.00004溫度試驗(yàn)點(diǎn)10℃p20溫度影響量允許值±0.00225MPa試驗(yàn)點(diǎn)（MPa）標(biāo)準(zhǔn)器讀數(shù)被校校驗(yàn)儀讀數(shù)p20溫度影響量（MPa）壓力標(biāo)準(zhǔn)值Ps（MPa）大氣壓（kPa）溫度標(biāo)準(zhǔn)值t(℃)p20理論（MPa）壓力pt（MPa）p20修正（MPa）正行程0.00.0000101.8860.46-0.012620.0000-0.01260.000020.20.2000101.8860.330.161120.19910.1603-0.000820.40.4000101.8860.290.332650.39930.3320-0.000650.60.6000101.8860.240.501850.59960.5015-0.000350.80.8000101.8860.200.668480.80000.66850.000020.90.9000101.8860.180.750610.90010.75080.00019反行程0.90.9000101.8860.180.750610.90010.75080.000190.80.8000101.8860.160.668590.79990.6685-0.000090.60.6000101.8860.040.502260.59940.5018-0.000460.40.4000101.8859.980.333670.39920.3330-0.000670.20.2000101.8859.300.161980.19910.1612-0.000780.00.0000101.8859.16-0.012260.0000-0.0123-0.00004溫度試驗(yàn)點(diǎn)60℃p20溫度影響量允許值±0.0036MPa（5）壓力控制項(xiàng)目：控制穩(wěn)定性、壓力控制超（回）調(diào)量、目標(biāo)壓力穩(wěn)定持續(xù)時(shí)間和控壓速率）試驗(yàn)點(diǎn)（MPa）控制穩(wěn)定性控制超（回）調(diào)量30s內(nèi)標(biāo)準(zhǔn)器最大值（MPa）30s內(nèi)標(biāo)準(zhǔn)器最小值（MPa）控制穩(wěn)定性（MPa）控制穩(wěn)定性允許值（MPa）達(dá)到穩(wěn)定中標(biāo)準(zhǔn)器最大（小）值（MPa）穩(wěn)定值（MPa）控制超（回）調(diào)量（MPa）超（回）調(diào)量允許值（MPa）0.20.19970.19940.000150.00090.20360.19970.00390.0020.50.49970.49910.00030.00090.50910.49970.00220.0050.80.80000.79890.000550.00090.80680.80000.00680.0080.80.79940.79900.00020.00090.79910.79930.00020.0080.50.49970.49920.000250.00090.49890.49970.00080.0050.20.19980.19970.00050.00090.19650.19970.00320.002目標(biāo)壓力穩(wěn)定持續(xù)時(shí)間：≥2min控壓速率控壓類型控壓起始點(diǎn)（MPa）測(cè)量點(diǎn)（MPa）時(shí)間（s）控壓速率（MPa/s）備注升壓0.38500.478654.480.0017檔位1降壓0.50200.460072.840.0006檔位1升壓0.46090.478918.870.0010檔位3降壓0.47200.460022.570.0005檔位3（6）密封性時(shí)間0min時(shí)間10min時(shí)間15min后5分鐘壓力下降值（MPa）密封性允許值（MPa）示值（MPa）示值（MPa）示值（MPa）0.85000.84990.84990.00000.0085

附件2試驗(yàn)設(shè)備名稱型號(hào)測(cè)量范圍準(zhǔn)確度等級(jí)或不確定度或最大允許誤差制造廠及出廠編號(hào)證書編號(hào)證書有效期至模塊式數(shù)字壓力校驗(yàn)儀PM200-G1M（0～1）MPa0.02級(jí)FLUKE/4022024RG2021X-0174872022.10.19二等標(biāo)準(zhǔn)鉑電阻溫度計(jì)（-189.3442～660.323）℃（-189.3442～660.323）℃二等FLUKE/30812020E11-20-24072530022022.04.08四通道便攜式測(cè)溫儀FLUKE1529(0～10000)Ω四線制電阻測(cè)量相對(duì)誤差≤3×10-5FLUKE/B11324DC2021B-0002452022.02.13制冷恒溫槽CJTL-80A（-80~95）℃均勻性：U=0.004℃（k=2）波動(dòng)性：U=0.006℃（k=2）湖州唯立儀表廠/6803RG2021X-0064572022.06.10高低溫試驗(yàn)箱C-20/200/S（-25～180）℃U

=

0.11℃（k=2）CTS/148090RG2021X-0181552022.06.15氣壓儀器檢定裝置QYJD2B(20～1100)hPa0.02級(jí)太原市太航壓力測(cè)試科技有限公司/09006RG2021X-0056892022.06.06電子秒表SJ9-2Ⅱ/MPE：±0.5s/d上海手表五廠/060345DC2021B-0028272022.06.03被檢樣品信息名稱準(zhǔn)確度等級(jí)或不確定度或最大允許誤差測(cè)量范圍型號(hào)編號(hào)生產(chǎn)廠家壓力產(chǎn)生方式SF6密度繼電器校驗(yàn)儀0.1級(jí)（0～1）MPaJHMD-3M-0249廈門加華電力科技有限公司內(nèi)部發(fā)生壓力試驗(yàn)環(huán)境溫度：（19.1～21.5）℃濕度：（35～42）%RH大氣壓：（101.4～102.1）kPa試驗(yàn)信息試驗(yàn)人員：賀曉輝沈燕春試驗(yàn)地點(diǎn)：合肥市包河區(qū)延安路13號(hào)安徽省計(jì)量科學(xué)研究院北樓A406、A411室試驗(yàn)時(shí)間：2021.12.19～2021.12.27試驗(yàn)數(shù)據(jù)（1）零位漂移：壓力顯示值（MPa）零位漂移（MPa）零位漂移允許值（MPa）時(shí)間0min時(shí)間15min時(shí)間30min時(shí)間45min時(shí)間60min0.00030.00020.00010.00010.00000.00030.0005說(shuō)明1：試驗(yàn)時(shí)間：2021.12.20試驗(yàn)環(huán)境條件：21.5℃、39%RH。（2）壓力示值誤差、回程誤差與重復(fù)性壓力標(biāo)準(zhǔn)器示值（MPa）校驗(yàn)儀壓力測(cè)量值（MPa）第一次第二次第三次正行程反行程正行程反行程正行程反行程0.00000.00000.00000.00000.00000.00000.00000.20000.20000.19990.20000.19980.19990.19980.40000.39970.39960.39970.39950.39950.39940.60000.59950.59930.59940.59930.59930.59920.80000.79930.79920.79920.79910.79920.79911.00000.99920.99920.99910.99900.99900.9990壓力示值誤差最大值：-0.0010MPa回程誤差最大值：0.0002MPa重復(fù)性最大值：0.0002MPa壓力示值誤差允許值：±0.001MPa回程誤差允許值：0.001MPa重復(fù)性允許值：0.001MPa說(shuō)明1：試驗(yàn)時(shí)間：2021.12.20試驗(yàn)環(huán)境條件：21.5℃、39%RH；說(shuō)明2：校準(zhǔn)方式為外接壓力標(biāo)準(zhǔn)（及壓力源）升降壓的的方式。（3）溫度示值誤差設(shè)定值-50℃-20℃20℃60℃80℃測(cè)量值（℃）（按標(biāo)準(zhǔn)-被校-被校-標(biāo)準(zhǔn)讀數(shù)，循環(huán)三次）標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器-50.0004-49.4-19.9777-19.219.961120.859.937561.179.921381.1-49.9999-49.4-19.9770-19.319.960620.859.939361.079.920681.0-50.0008-49.4-19.9773-19.219.961420.859.938761.179.920881.1-50.0015-49.4-19.9783-19.219.961620.859.938561.079.921881.1-50.0004-49.4-19.9785-19.319.961220.859.939661.179.921781.1-50.0013-49.4-19.9777-19.219.960920.859.938861.179.921681.0平均值（℃）-50.0007-49.4-19.9778-19.219.961120.859.938761.179.921381.1誤差值（℃）0.60.60.81.21.2說(shuō)明1：試驗(yàn)時(shí)間：2021.12.21試驗(yàn)環(huán)境條件：19.1℃、42%RH說(shuō)明2：校驗(yàn)儀技術(shù)說(shuō)明書標(biāo)示溫度測(cè)量范圍為（-50～100）℃，實(shí)際測(cè)量過(guò)程中測(cè)溫傳感器高于約85℃時(shí)，校驗(yàn)儀顯示端未能正常顯示溫度量值，故本次試驗(yàn)選?。?50～80）℃內(nèi)較均勻的5個(gè)試驗(yàn)點(diǎn)（即包括測(cè)量下限、但不包括測(cè)量上限）。（4）p20溫度影響量試驗(yàn)點(diǎn)（MPa）標(biāo)準(zhǔn)器讀數(shù)被校校驗(yàn)儀讀數(shù)p20溫度影響量（MPa）壓力標(biāo)準(zhǔn)值Ps（MPa）大氣壓（kPa）溫度標(biāo)準(zhǔn)值t(℃)p20理論（MPa）壓力pt（MPa）p20修正（MPa）正行程0.00.0000101.35-24.810.120350.00450.12050.000150.20.2000101.36-24.790.362460.20840.36330.000840.40.4000101.36-24.780.612080.40970.6104-0.001680.60.6000101.36-24.820.871910.61110.8680-0.003910.80.8000101.36-24.791.145580.81281.1402-0.005381.01.0000101.36-24.781.441741.01361.3605-0.08124反行程1.01.0000101.36-24.751.441391.01361.3606-0.080790.80.8000101.36-24.771.145430.81271.1403-0.005130.60.6000101.36-24.790.871760.61110.8681-0.003660.40.4000101.36-24.780.612080.40960.6107-0.001380.20.2000101.36-24.760.362410.20830.36370.001290.00.0000101.36-24.760.120330.00460.12090.00057溫度試驗(yàn)點(diǎn)-25℃p20溫度影響量允許值±0.00325MPa試驗(yàn)點(diǎn)（MPa）標(biāo)準(zhǔn)器讀數(shù)被校校驗(yàn)儀讀數(shù)p20溫度影響量（MPa）壓力標(biāo)準(zhǔn)值Ps（MPa）大氣壓（kPa）溫度標(biāo)準(zhǔn)值t(℃)p20理論（MPa）壓力pt（MPa）p20修正（MPa）正行程0.00.0000101.8059.910.089340.00000.09000.000660.20.2000101.8059.920.263310.19350.2601-0.003210.40.4000101.8059.930.435080.38990.4286-0.006480.60.6000101.8059.930.604510.58680.5952-0.009310.80.8000101.8159.920.771430.78340.7590-0.012431.01.0000101.8159.890.935680.96320.9042-0.03148反行程1.01.0000101.8059.890.935670.96290.9042-0.031470.80.8000101.8059.890.771510.78180.7589-0.012610.60.6000101.8059.900.604570.58560.5953-0.009270.40.4000101.8059.900.435120.38920.4287-0.006420.20.2000101.8059.910.263320.19340.2601-0.003220.00.0000101.8059.900.089350.00000.09010.00075溫度試驗(yàn)點(diǎn)60℃p20溫度影響量允許值±0.003MPa說(shuō)明1：試驗(yàn)時(shí)間：2021.12.23試驗(yàn)環(huán)境條件：20.1℃、37%RH說(shuō)明2：此表格中錄入的大氣壓數(shù)據(jù)來(lái)自于氣壓儀器檢定裝置（編號(hào)09006），而未采用校驗(yàn)儀本身實(shí)際顯示值。試驗(yàn)過(guò)程中校驗(yàn)儀實(shí)際顯示值為：-25℃試驗(yàn)點(diǎn)：0.1019MPaabs；60℃試驗(yàn)點(diǎn)：0.1020MPaabs。說(shuō)明3：本項(xiàng)試驗(yàn)對(duì)部分校驗(yàn)儀存在一定高、低溫影響下壓力示值變化的可能。（5）壓力控制項(xiàng)目：控制穩(wěn)定性、壓力控制超（回）調(diào)量、目標(biāo)壓力穩(wěn)定持續(xù)時(shí)間和控壓速率）試驗(yàn)點(diǎn)（MPa）控制穩(wěn)定性控制超（回）調(diào)量30s內(nèi)標(biāo)準(zhǔn)器最大值（MPa）30s內(nèi)標(biāo)準(zhǔn)器最小值（MPa）控制穩(wěn)定性（MPa）控制穩(wěn)定性允許值（MPa）達(dá)到穩(wěn)定中標(biāo)準(zhǔn)器最大值（MPa）穩(wěn)定值（MPa）控制超（回）調(diào)量（MPa）超（回）調(diào)量允許值（MPa）0.10.100080.100070.0000050.00050.100790.100070.000720.0010.20.200060.200050.0000050.00050.200630.200060.000570.0020.40.400110.399940.0000850.00050.400970.400110.000860.0040.60.600160.600120.0000200.00050.601470.600160.001310.0060.80.800190.800140.0000250.00050.801090.80020.000890.0080.90.900100.900070.0000150.00050.902250.900270.001980.0090.90.900570.900530.0000200.00050.902620.900400.002220.0090.80.801470.801360.0000550.00050.801160.801470.000310.0080.60.601680.601630.0000250.00050.601540.601700.000160.0060.40.401190.401150.0000200.00050.398500.401080.002580.0040.20.200700.200630.0000350.00050.200270.200730.000460.0020.10.100690.100640.0000250.00050.100590.100750.000160.001目標(biāo)壓力穩(wěn)定持續(xù)時(shí)間：≥2min說(shuō)明1：試驗(yàn)時(shí)間：2021.12.27試驗(yàn)環(huán)境條件：21.3℃、35%RH說(shuō)明2：本項(xiàng)試驗(yàn)數(shù)據(jù)是在p20溫度影響量試驗(yàn)后，示值產(chǎn)生負(fù)偏移并進(jìn)行示值調(diào)整后測(cè)得。說(shuō)明3：本項(xiàng)試驗(yàn)校驗(yàn)儀控壓起始點(diǎn)不能通過(guò)設(shè)置選取，同時(shí)也無(wú)SF6密度控制器來(lái)模擬接點(diǎn)動(dòng)作校驗(yàn)過(guò)程，因此控壓速率試驗(yàn)未進(jìn)行。（6）密封性時(shí)間0min時(shí)間10min時(shí)間15min后5分鐘壓力下降值（MPa）密封性允許值（MPa）示值（MPa）示值（MPa）示值（MPa）0.99980.99740.98690.00050.010.99980.99440.99340.00100.010.99910.99690.99620.00070.01說(shuō)明1：試驗(yàn)時(shí)間：2021.12.27試驗(yàn)環(huán)境條件：21.3℃、35%RH

附件3試驗(yàn)設(shè)備名稱型號(hào)測(cè)量范圍準(zhǔn)確度等級(jí)或不確定度或最大允許誤差數(shù)字壓力控制器PPC3（0~2）MPa（abs）0.01級(jí)四通道數(shù)字測(cè)溫儀/（0~100）mV(0.1~1000)Ω0.005%標(biāo)準(zhǔn)鉑電阻溫度計(jì)/（-189.3442~419.527）℃二等大氣壓力計(jì)JCD-33（30.0~110.0）kPa0.3%FS秒表SJ9-2Ⅱ/MPE：±0.5s/d被檢樣品信息名稱準(zhǔn)確度等級(jí)或不確定度或最大允許誤差測(cè)量范圍型號(hào)編號(hào)生產(chǎn)廠家壓力產(chǎn)生方式SF6密度繼電器校驗(yàn)儀0.2級(jí)（0~0.9）MPaJD-12JD1212020731鄭州賽奧電子股份有限公司自動(dòng)試驗(yàn)環(huán)境溫度：20.9℃濕度：34%RH大氣壓：102.48kPa試驗(yàn)信息試驗(yàn)人員：陳昊王尊駱麗郭振梁潘明芳試驗(yàn)地點(diǎn)：浙江電科院503壓力實(shí)驗(yàn)室試驗(yàn)時(shí)間：2021.12.13～2021.12.31試驗(yàn)數(shù)據(jù)（1）零位漂移：壓力顯示值（MPa）零位漂移（MPa）零位漂移允許值（MPa）時(shí)間0min時(shí)間15min時(shí)間30min時(shí)間45min時(shí)間60min0.00000.00000.00000.00000.00000.00000.0009（2）壓力示值誤差、回程誤差與重復(fù)性壓力標(biāo)準(zhǔn)器示值（MPa）校驗(yàn)儀壓力測(cè)量值（MPa）第一次第二次第三次正行程反行程正行程反行程正行程反行程0.00000.00000.00000.00000.00000.00000.00000.10000.10060.10050.10050.10040.10040.10040.20000.20060.20060.20050.20050.20050.20040.30000.30060.30060.30050.30040.30040.30040.40000.40060.40050.40040.40040.40040.40040.50000.50060.50060.50050.50050.50040.50050.60000.60060.60060.60050.60050.60050.60040.70000.70050.70060.70040.70040.70040.70040.80000.80060.80060.80050.80050.80050.80040.90000.90060.90050.90050.90050.90040.9004壓力示值誤差最大值：0.0006MPa回程誤差最大值：0.0001MPa重復(fù)性最大值：0.0002MPa壓力示值誤差允許值：±0.0018MPa回程誤差允許值：0.0018MPa重復(fù)性允許值：0.0018MPa（3）溫度示值誤差說(shuō)明：被檢儀器自帶溫度傳感器為內(nèi)置溫度傳感器，溫度示值誤差未檢。（4）p20溫度影響量試驗(yàn)點(diǎn)（MPa）標(biāo)準(zhǔn)器讀數(shù)被校校驗(yàn)儀讀數(shù)p20溫度影響量（MPa）壓力標(biāo)準(zhǔn)值Ps（MPa）大氣壓（kPa）溫度標(biāo)準(zhǔn)值t(℃)p20理論（MPa）壓力pt（MPa）p20修正（MPa）正行程0.00.0000102.86-10.060.012170.00180.01420.002030.20.2000102.86-10.070.238450.20320.24370.005250.40.4000102.86-10.060.468770.40330.47860.009830.60.6000102.86-10.060.704190.60340.72160.017410.80.8000102.86-10.060.946220.80360.97640.030180.90.9000102.86-10.071.070490.90371.09000.01951反行程0.90.9000102.86-10.071.070490.90371.09000.019510.80.8000102.86-10.060.946220.80370.97650.030280.60.6000102.86-10.060.704190.60350.72170.017510.40.4000102.86-10.050.468750.40340.47870.009950.20.2000102.86-10.050.238420.20330.24380.005380.00.0000102.86-10.050.012160.00180.01420.00204溫度試驗(yàn)點(diǎn)-10℃p20溫度影響量允許值±0.00315MPa試驗(yàn)點(diǎn)（MPa）標(biāo)準(zhǔn)器讀數(shù)被校校驗(yàn)儀讀數(shù)p20溫度影響量（MPa）壓力標(biāo)準(zhǔn)值Ps（MPa）大氣壓（kPa）溫度標(biāo)準(zhǔn)值t(℃)p20理論（MPa）壓力pt（MPa）p20修正（MPa）正行程0.00.0000102.7840.36-0.006840.00000.00000.006840.20.2000102.7840.360.178870.19920.1777-0.001170.40.4000102.7840.340.363210.39920.3610-0.002210.60.6000102.7840.340.545970.59920.5423-0.003670.80.8000102.7840.350.726970.79930.7215-0.005470.90.9000102.7840.350.816770.89930.8101-0.00667反行程0.90.9000102.7840.350.816770.89930.8101-0.006670.80.8000102.7840.370.726910.79940.7216-0.005310.60.6000102.7840.390.545850.59930.5424-0.003450.40.4000102.7840.400.363110.39920.3610-0.002110.20.2000102.7840.390.178840.19920.1777-0.001140.00.0000102.7840.40-0.006850.00000.00000.00685溫度試驗(yàn)點(diǎn)40℃p20溫度影響量允許值±0.0027MPa（5）壓力控制項(xiàng)目：控制穩(wěn)定性、壓力控制超（回）調(diào)量、目標(biāo)壓力穩(wěn)定持續(xù)時(shí)間和控壓速率）試驗(yàn)點(diǎn)（MPa）控制穩(wěn)定性控制超（回）調(diào)量30s內(nèi)標(biāo)準(zhǔn)器最大值（MPa）30s內(nèi)標(biāo)準(zhǔn)器最小值（MPa）控制穩(wěn)定性（MPa）控制穩(wěn)定性允許值（MPa）達(dá)到穩(wěn)定中標(biāo)準(zhǔn)器最大（?。┲担∕Pa）穩(wěn)定值（MPa）控制超（回）調(diào)量（MPa）超（回）調(diào)量允許值（MPa）0.20.197020.196990.000020.00090.197230.197050.000180.0020.50.496450.496340.000050.00090.497080.496320.000760.0050.80.797450.797330.000060.00090.798310.797360.000950.0080.80.800400.800360.000020.00090.800370.800360.000010.0080.50.501030.500960.000040.00090.501050.501070.000020.0050.20.198880.198830.000020.00090.198440.198830.000390.002目標(biāo)壓力穩(wěn)定持續(xù)時(shí)間：≥2min控壓速率控壓類型控壓起始點(diǎn)（MPa）測(cè)量點(diǎn)（MPa）時(shí)間（s）控壓速率（MPa/s）備注升壓0.4550.47610.940.0019/降壓0.4890.45522.570.0015/（6）密封性時(shí)間0min時(shí)間10min時(shí)間15min后5分鐘壓力下降值（MPa）密封性允許值（MPa）示值（MPa）示值（MPa）示值（MPa）0.88250.86340.85710.00630.0088

附件4試驗(yàn)設(shè)備名稱型號(hào)測(cè)量范圍準(zhǔn)確度等級(jí)或不確定度或最大允許誤差數(shù)字壓力控制器PPC3（0~2）MPa（abs）0.01級(jí)四通道數(shù)字測(cè)溫儀/（0~100）mV(0.1~1000)Ω0.005%標(biāo)準(zhǔn)鉑電阻溫度計(jì)/（-189.3442~419.527）℃二等大氣壓力計(jì)JCD-33（30.0~110.0）kPa0.3%FS秒表SJ9-2Ⅱ/MPE：±0.5s/d被檢樣品信息名稱準(zhǔn)確度等級(jí)或不確定度或最大允許誤差測(cè)量范圍型號(hào)編號(hào)生產(chǎn)廠家壓力產(chǎn)生方式SF6密度繼電器校驗(yàn)儀0.2級(jí)（0~0.9）MPaJD-12/鄭州賽奧電子股份有限公司自動(dòng)試驗(yàn)環(huán)境溫度：21.9℃濕度：56%RH大氣壓：101.30kPa試驗(yàn)信息試驗(yàn)人員：楊青陳昊王尊郭振梁潘明芳試驗(yàn)地點(diǎn)：浙江電科院503壓力實(shí)驗(yàn)室試驗(yàn)時(shí)間：2020.1試驗(yàn)數(shù)據(jù)（1）零位漂移：壓力顯示值（MPa）零位漂移（MPa）零位漂移允許值（MPa）時(shí)間0min時(shí)間15min時(shí)間30min時(shí)間45min時(shí)間60min0.00020.00020.00030.00030.00030.00010.0009（2）壓力示值誤差、回程誤差與重復(fù)性壓力標(biāo)準(zhǔn)器示值（MPa）校驗(yàn)儀壓力測(cè)量值（MPa）第一次第二次第三次正行程反行程正行程反行程正行程反行程0.00000.00030.00030.00030.00040.00030.00030.10000.10030.10040.10030.10040.10040.10040.20000.20020.20020.20020.20030.20020.20030.30000.30020.30020.30020.30020.30020.30030.40000.40010.40010.40010.40010.40010.40020.50000.50020.50020.50020.50020.50020.50020.60000.60030.60030.60030.60030.60030.60030.70000.70030.70030.70030.70030.70030.70030.80000.80040.80040.80040.80040.80040.80040.90000.90040.90040.90040.90040.90040.9004壓力示值誤差最大值：0.0004MPa回程誤差最大值：0.0001MPa重復(fù)性最大值：0.0001MPa壓力示值誤差允許值：±0.0018MPa回程誤差允許值：0.0018MPa重復(fù)性允許值：0.0018MPa（3）溫度示值誤差說(shuō)明：被檢儀器自帶溫度傳感器為內(nèi)置溫度傳感器，溫度示值誤差未檢。（4）p20溫度影響量試驗(yàn)點(diǎn)（MPa）標(biāo)準(zhǔn)器讀數(shù)被校校驗(yàn)儀讀數(shù)p20溫度影響量（MPa）壓力標(biāo)準(zhǔn)值Ps（MPa）大氣壓（kPa）溫度標(biāo)準(zhǔn)值t(℃)p20理論（MPa）壓力pt（MPa）p20修正（MPa）正行程0.20.2000101.86-19.710.35490.19810.35220.00270.40.4000101.86-19.720.59760.39800.59450.00310.50.5000101.86-19.700.72190.49820.71870.00320.60.6000101.86-19.710.84860.59750.84420.00440.80.8000101.86-19.701.11080.79801.10600.0048反行程0.80.8000101.86-19.701.01080.79801.10600.00480.60.6000101.86-19.680.84840.59830.84520.00320.50.5000101.86-19.690.72190.49840.71900.00290.40.4000101.86-19.700.59760.39810.59460.00300.20.2000101.86-19.720.35490.19810.35220.0027溫度試驗(yàn)點(diǎn)-20℃p20溫度影響量允許值±0.0036MPa試驗(yàn)點(diǎn)（MPa）標(biāo)準(zhǔn)器讀數(shù)被校校驗(yàn)儀讀數(shù)p20溫度影響量（MPa）壓力標(biāo)準(zhǔn)值Ps（MPa）大氣壓（kPa）溫度標(biāo)準(zhǔn)值t(℃)p20理論（MPa）壓力pt（MPa）p20修正（MPa）正行程0.20.2000102.3760.330.26350.19950.26350.00000.40.4000102.3760.270.43500.39950.43500.00000.50.5000102.3760.220.51990.49960.52000.00030.60.6000102.3759.300.60610.60000.60470.00140.80.8000102.3760.440.77010.80020.77150.0014反行程0.80.8000102.3760.440.77010.80020.77150.00010.60.6000102.3760.320.60400.59980.60450.00050.50.5000102.3760.260.51980.49980.52020.00010.40.4000102.3760.220.43510.39970.43520.00030.20.2000102.3760.200.26350.20000.26380.0003溫度試驗(yàn)點(diǎn)60℃p20溫度影響量允許值±0.0036MPa（5）壓力控制項(xiàng)目：控制穩(wěn)定性、壓力控制超（回）調(diào)量、目標(biāo)壓力穩(wěn)定持續(xù)時(shí)間和控壓速率）試驗(yàn)點(diǎn)（MPa）控制穩(wěn)定性控制超（回）調(diào)量30s內(nèi)標(biāo)準(zhǔn)器最大值（MPa）30s內(nèi)標(biāo)準(zhǔn)器最小值（MPa）控制穩(wěn)定性（MPa）控制穩(wěn)定性允許值（MPa）達(dá)到穩(wěn)定中標(biāo)準(zhǔn)器最大（?。┲担∕Pa）穩(wěn)定值（MPa）控制超（回）調(diào)量（MPa）超（回）調(diào)量允許值（MPa）0.20.20000.19710.19700.00010.00090.19710.19710.00000.60.59680.59680.00000.00090.59690.59680.00010.0060.80.79670.79650.00020.00090.79710.79670.00040.0080.80.80110.80110.00000.00090.80110.80110.00000.0080.60.60190.60170.00020.00090.60160.60170.00010.0060.20.20050.20040.00010.00090.20040.20040.00000.002目標(biāo)壓力穩(wěn)定持續(xù)時(shí)間：≥2min控壓速率控壓類型控壓起始點(diǎn)（MPa）測(cè)量點(diǎn)（MPa）時(shí)間（s）控壓速率（MPa/s）備注升壓0.4520.47013.980.0013/降壓0.4800.44921.920.0014/（6）密封性時(shí)間0min時(shí)間10min時(shí)間15min后5分鐘壓力下降值（MPa）密封性允許值（MPa）示值（MPa）示值（MPa）示值（MPa）0.89650.89640.89650.00010.009

附件5試驗(yàn)設(shè)備名稱型號(hào)測(cè)量范圍準(zhǔn)確度等級(jí)或不確定度或最大允許誤差氣體活塞式壓力計(jì)PG7601(-0.1-7)MPa0.005級(jí)標(biāo)準(zhǔn)鉑電阻溫度計(jì)WZPB-1-189.344℃~660.323℃一等標(biāo)準(zhǔn)數(shù)字多用表34420A10-3Ω~105Ω±0.003%大氣壓力計(jì)JCD-33（30.0~110.0）kPa0.3%FS秒表SJ9-2Ⅱ/MPE：±0.5s/d被檢樣品信息名稱準(zhǔn)確度等級(jí)或不確定度或最大允許誤差測(cè)量范圍型號(hào)編號(hào)生產(chǎn)廠家壓力產(chǎn)生方式六氟化硫密度繼電器校驗(yàn)儀0.1級(jí)（0~0.9）MPaFMC-9Tc17037028b西安亞能電氣有限責(zé)任公司自動(dòng)試驗(yàn)環(huán)境溫度：19.0℃濕度：37%RH大氣壓：97.79kPa試驗(yàn)信息試驗(yàn)人員：王志浩、楊海燕、趙蒙、原晨婧試驗(yàn)地點(diǎn)：陜西省西安市閻良區(qū)長(zhǎng)空路1599號(hào)試驗(yàn)時(shí)間：2022年2月24日試驗(yàn)數(shù)據(jù)（1）零位漂移：壓力顯示值（MPa）零位漂移（MPa）零位漂移允許值（MPa）時(shí)間0min時(shí)間15min時(shí)間30min時(shí)間45min時(shí)間60min0.00000.00010.00000.00000.00010.00010.00045（2）壓力示值誤差、回程誤差與重復(fù)性壓力標(biāo)準(zhǔn)器示值（MPa）校驗(yàn)儀壓力測(cè)量值（MPa）第一次第二次第三次正行程反行程正行程反行程正行程反行程0.00.00000.00030.00000.00030.00000.00000.10.10030.10040.10040.10030.10040.10050.20.20040.20040.20050.20040.20050.20060.30.30050.30060.30050.30050.30060.30070.40.40030.40050.40040.40040.40040.40040.50.50040.50040.50040.50030.50040.50050.60.60040.60040.60050.60040.60050.60060.70.70030.70040.70040.70040.70040.70050.80.80040.80040.80040.80040.80050.80050.90.90060.90060.90050.90050.90060.9006壓力示值誤差最大值：0.0007MPa回程誤差最大值：0.0001MPa重復(fù)性最大值：0.0002MPa壓力示值誤差允許值：±0.0009MPa回程誤差允許值：0.0009MPa重復(fù)性允許值：0.0009MPa（3）溫度示值誤差設(shè)定值-30℃0℃20℃40℃60℃測(cè)量值（℃）（按標(biāo)準(zhǔn)-被校-被校-標(biāo)準(zhǔn)讀數(shù)，循環(huán)三次）標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器23.4592-20.0624.4791-9.9625.49420.0026.507810.0027.517720.1623.4592-20.0624.4791-9.9625.49420.0026.507810.0227.517920.1423.4592-20.0624.4791-9.9825.49410.0026.507510.0227.517920.1623.4593-20.0424.4791-9.9625.49410.0026.507510.0227.517920.1623.4593-20.0624.4791-9.9625.49410.0026.507710.0227.517920.1423.4592-20.0424.4791-9.9625.49420.0026.507710.0227.517920.16平均值（℃）-19.9703-20.05-9.98474-9.96-0.016060.009.96817410.0219.9501720.15誤差值（℃）-0.07970.024740.016060.0518260.19983設(shè)定值30℃40℃50℃60℃測(cè)量值（℃）（按標(biāo)準(zhǔn)-被校-被校-標(biāo)準(zhǔn)讀數(shù)，循環(huán)三次）標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器標(biāo)準(zhǔn)器被校器28.524530.2629.528540.2630.530250.2831.529060.3328.524430.2629.528540.2830.530350.2831.529060.3428.524330.2629.528540.2630.530350.2831.529060.3428.524330.2629.528540.2630.530450.2831.529060.3328.524430.2629.528540.2830.530350.2831.529060.3428.524430.2629.528540.2830.530450.2831.529060.34平均值（℃）29.9261630.2639.9087840.2749.8990250.2859.8885460.34誤差值（℃）0.333840.361220.380980.45146（4）p20溫度影響量試驗(yàn)點(diǎn)（MPa）標(biāo)準(zhǔn)器讀數(shù)被校校驗(yàn)儀讀數(shù)p20溫度影響量（MPa）壓力標(biāo)準(zhǔn)值Ps（MPa）大氣壓（kPa）溫度標(biāo)準(zhǔn)值t(℃)p20理論（MPa）壓力pt（MPa）p20修正（MPa）正行程0.10.1000098.44-19.330.133090.10010.13350.046%0.30.3000098.44-19.330.371890.30020.37280.101%0.50.5000098.44-19.330.617660.50010.61860.104%0.70.7000098.44-19.330.872690.70010.87390.134%0.90.9000098.44-19.331.140910.90021.14220.143%反行程0.90.9000098.44-19.331.140910.90021.14210.132%0.70.7000098.44-19.330.872690.70010.87400.146%0.50.5000098.44-19.330.617660.50000.61850.093%0.30.3000098.44-19.330.371890.30030.37300.123%0.10.1000098.44-19.330.133090.10010.13360.057%溫度試驗(yàn)點(diǎn)-20℃p20溫度影響量允許值±0.3%試驗(yàn)點(diǎn)（MPa）標(biāo)準(zhǔn)器讀數(shù)被校校驗(yàn)儀讀數(shù)p20溫度影響量（MPa）壓力標(biāo)準(zhǔn)值Ps（MPa）大氣壓（kPa）溫度標(biāo)準(zhǔn)值t(℃)p20理論（MPa）壓力pt（MPa）p20修正（MPa）正行程0.10.1000098.4460.020.075160.10010.0751-0.007%0.30.3000098.4460.020.247980.30030.24800.002%0.50.5000098.4460.020.418510.50020.4185-0.001%0.70.7000098.4460.020.586540.70020.5864-0.016%0.90.9000098.4460.020.751880.90030.75190.002%反行程0.90.9000098.4460.020.751880.90030.75200.013%0.70.7000098.4460.020.586540.70030.5865-0.004%0.50.